000 02198 a2200145 4500
003 DZ-ElOued
005 20260602171157.0
100 1 _aCherbi, Bachir
245 0 0 _aEtude de l'effet du pHde millieu réactionnel sur les propriétés des nanoparticules d'oxyde mérallique obtenue par méthode verte
260 _b
_c2024
500 _aEtude de l'effet du pHde millieu réactionnel sur les propriétés des nanoparticules d'oxyde mérallique obtenue par méthode verte
520 _aThis study explores an eco-friendly approach to synthesizing zinc oxide (ZnO) nanoparticles using plant extracts as an alternative to conventional physical or chemical methods. ZnO nanoparticles were produced via a green synthesis process using Portulaca oleracea (purslane) leaf extract at varying pH levels of 4, 6, 9.5, and 11. The impact of pH on the optical and structural characteristics of the synthesized nanoparticles was investigated. Ultraviolet-visible (UV-Vis) spectrophotometry and Fourier-transform infrared (FTIR) spectroscopy techniques were employed to analyze the optical properties, while scanning electron microscopy (SEM) and X-ray diffraction (XRD) were utilized to study the structural properties. Additionally, the photocatalytic performance of the synthesized ZnO nanoparticles was evaluated through the degradation of methyl orange dye. The characterization results confirmed the successful biosynthesis of ZnO nanoparticles with sizes ranging from 22.17 to 27.38 nm. UV-Vis analysis revealed maximum absorption in the 350-380 nm range, indicative of the Zn-O bond. FTIR spectra exhibited a distinct peak at 474 cm-1, attributed to Zn-O vibrations. SEM images revealed that the obtained nanoparticles generally exhibited spherical or oval morphologies. The synthesis pH significantly influenced the optical and morphological properties of the ZnO nanoparticles. The results demonstrated the high performance of the green-synthesized ZnO nanoparticles in dye degradation applications.
650 4 _a/Etude//de//l//effet//du//pHde//millieu//rǎctionnel//sur//les//propriťš//des//nanoparticules//d//oxyde//mřallique//obtenue//par//mťhode//verte/
942 _cTHESIS
999 _c16976
_d16976